Electron spectroscopy

The Multilab/Argus Electron Spectrometer includes Selected-area and Imaging X-ray Photoelectron Spectroscopy (SAXPS/iXPS). The UHV system is modular including also preparation chambers equipped with various sample preparation facilities.


Multilab/Argus Electron Spectrometer at a glance

Measurement modes
  • X-ray Photoelectron Spectroscopy (XPS)
    • Selected-area XPS (SAXPS)
    • Imaging XPS (iXPS)
  • X-ray Auger Electron Spectroscopy (XAES)
Aperture/
Analysis area/
Lateral resolution/
Typical application
  • A1 / ∅ 0.066 mm / 54 μm / High resolution iXPS
  • A2 / ∅0.198 mm / 136 μm / Medium resolution iXPS
  • A3 / 0.311 × 3.22 mm² / Snapshot mode
  • A4 / ∅ 1.93 mm / 1.11 mm / SAXPS
  • A5 / 1.54 × 4.09 mm² / High count rate SAXPS
  • A6 / 1.23 × 4.66 mm² / Maximum count rate SAXPS
Exitation sources
  • Al Kα X-ray source (1486.6 eV)
  • Mg Kα X-ray source (1253.6 eV)
Analyser and detector
  • Argus hemispherical electron analyser
  • Microchannel plate electron multipliers and a 128 channel stripe anode detector
Sample preparation
options
  • Ar ion sputtering for surface cleaning and depth profiling
  • Activated nitrogen ion bombardment
  • Gas exposure (O2, H2O, air etc.)
  • Oxidation/Reduction
  • Physical vapour deposition (PVD)
  • Electrospraying
  • Annealing up to 800 °C (also during XPS measurement)
Sample
dimesions
  • Diameter: up to 1″
  • Thickness: <5 mm
  • Holder also for powder samples